I have a list. I want add a column for list with this format :
How to set this Validate for column?
i use this link , but don't work for me.
You've got a few options.
It DOES work if done correctly and is probably the quickest way do this.
2) A custom column that applies regular expression validation.
You can use/adapt one of these open source projects
3) Write your own custom column.
More complex - but allows you to combine server side and client side validation.
Though not as easy or powerful as regular expressions, standard Column Validation can use a rich selection of Excel-like string functions. For example...
Some more complex examples are described at http://sharepointsolutions.com/sharepoint-help/blog/2011/12/how-to-use-or-type-options-in-sharepoint-2010-column-validation/